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Beilstein J. Org. Chem. 2019, 15, 1257–1261, doi:10.3762/bjoc.15.122
Graphical Abstract
Figure 1: BN-phenanthrene 1a and synthesis of substituted derivatives proposed in this work.
Scheme 1: Synthesis of Cl-substituted BN-phenanthrene 1b.
Scheme 2: Palladium-catalyzed cross-couplings of Cl-substituted BN-phenanthrene 1b.
Scheme 3: Pd-catalyzed Sonogashira reactions of Cl-substituted BN-phenanthrene 1b.
Figure 2: UV–vis absorption (top) and emission (bottom) spectra for BN-phenanthrenes 1 and 5 in cyclohexane (...
Figure 3: Solutions of 1a–f and 5 (from left to right) under UV irradiation.
Beilstein J. Org. Chem. 2013, 9, 2242–2249, doi:10.3762/bjoc.9.263
Scheme 1: Gold(I)-catalyzed reactions of 1,6-enynes.
Scheme 2: Cyclization of o-(alkynyl)-(3-methylbut-2-enyl)benzenes 1. Previous work and proposed pathways.
Scheme 3: Synthesis of o-(alkynyl)-(3-methylbut-2-enyl)benzenes 1.
Scheme 4: Gold(I)-catalyzed cycloisomerization of 1a.
Scheme 5: Initial experiments and proof of concept.
Scheme 6: Gold(I)-catalyzed hydroxycyclization of enynes 1m,n.
Scheme 7: Gold(I)-catalyzed methoxycyclization of selected 1,6-enynes 1 [45].
Scheme 8: Labelling experiment and proposed mechanism.
Beilstein J. Org. Chem. 2011, 7, 786–793, doi:10.3762/bjoc.7.89
Scheme 1: Formation of 3-(inden-2-yl)indoles 3 and 4 from 3-propargylindoles. Energy barriers (kcal/mol) for ...
Scheme 2: Tandem 1,2-indole migration/aura-Nazarov cyclization from 3-propargylindoles bearing an aromatic su...
Figure 1: ORTEP diagram for 4a. Ellipsoids are shown at 30% level (hydrogen atoms are omitted for clarity).
Scheme 3: Comparison of the reactivity of C-2 substituted indoles 1j and 1k. Conditions: a) (Ph3P)AuCl/AgSbF6...
Scheme 4: Reactions of 3-propargylindoles 1l and 1m with bulky alkyl substituents at the propargylic position...